[Solid and liquid wastes from industrial processes: Innovations in material recovery and environmental protection] Lithium Recycling from Used Li-ion Batteries using Innovative Electrodialysis with Lithium Ionic conductor Lithium Recycling from Used Li-ion Batteries using Innovative Electrodialysis with Lithium Ionic conductor Tsuyoshi Hoshino1; 1ROKKASHO FUSION ENERGY RESEARCH CENTRE, Rokkasho-mura, Kamikita-gun, Japan; PAPER: 100/Electrochemistry/Invited (Oral) SCHEDULED: 12:35/Tue./Copacabana B (150/1st) ABSTRACT: In recent years, the industrial importance of lithium (Li) has increased due to its use in Li-ion batteries. Previously, the author had developed a method for the recovery of Li from seawater using a Li ionic superconductor functioning as a Li-ion separation membrane (LISM). In this method, only Li ions were successfully recovered from seawater through the LISM. Consequently, the author then developed a new innovative method for recycling Li from used Li-ion batteries using the LISM. This innovative method involves the use of an LISM, whereby only Li ions in a solution of used Li-ion batteries permeate from the positive electrode side to the negative electrode side during electrodialysis; the other ions, including Co, Al, and F, do not permeate the membrane. Li<sub>0.29</sub>La<sub>0.57</sub>TiO<sub>3</sub> was selected as the LISM. The positive side of the dialysis cell was filled with used Li-ion battery solution. Then the negative side was filled with distilled water. The applied dialysis voltage was 5 V, and electrode area was 16 cm2. The Li recovery ratio increased with electrodialysis time. Subsequently, Co, Al, and F were not permeated. After electrodialysis, CO<sub>2</sub> gas was bubbled in the Li recovery water to produce lithium carbonate (Li<sub>2</sub>CO<sub>3</sub>) as a raw material for Li-ion batteries. The Li<sub>2</sub>CO<sub>3</sub> deposition was easily generated by the reaction of CO<sub>2</sub> gas and the Li recovery solution as a lithium hydroxide (LiOH) solution. This new method for recycling Li-ion batteries shows good energy efficiency and is easily scalable. Thus, this electrodialysis method is suitable for the recovery of Li from used Li-ion batteries. References: [1] T. Hoshino, Desalination, 359, 59-63 (2015). |